How can the yield of epichlorohydrin produced by the glycerol method be increased?

2021-03-22View Original

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The yield of the finished product has been around 99.68 in recent days, with 0.22% recomposed components present; neither increasing the reflux flow nor reducing the feed rate or the steam supplied to the reboiler has had any effect! Even during the shutdown for inspection, no tray was lost in the tower; a few trays did break, and they were replaced, but that didn’t solve the problem. I’d like to ask the experts, can someone tell me?

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How can the yield of epichlorohydrin produced by the glycerol method be increased?

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