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After the low-pressure methanol catalyst is installed, can the methanol synthesis tower be press-tested with hydrogen or a mixture of hydrogen and nitrogen?

2017-03-27 View Original

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After the low-pressure methanol catalyst is installed, can the methanol synthesis tower be press-tested with hydrogen or a mixture of hydrogen and nitrogen? Recently, a company in Jiangsu was preparing to conduct pressure testing on its low-pressure methanol synthesis tower after catalyst loading. Due to the lack of medium-pressure nitrogen, it was decided to use hydrogen-nitrogen gas (ammonia synthesis gas) for pressurization; however, the catalyst manufacturer firmly opposed this approach. Please discuss what consequences using hydrogen and nitrogen gas will have on pressure
Reply #2 2017-03-27
The synthetic catalyst should not be able to use air
Reply #3 2017-03-27
Can hydrogen or a mixture of hydrogen and nitrogen be used for pressure testing? Please pay close attention to the question in the stem
Reply #4 2017-03-27
This post was last edited by he*aoyu8911 on 2017-3-27 at 15:08. Air should work, nitrogen as well; as for hydrogen, its concentration during reduction is less than 0.2%. If you introduce it at such an early stage, are you sure it can be completely displaced during reduction? The catalyst has a porous structure with an extremely large specific surface area~~
Reply #5 2017-03-28
Nitrogen should be used for pressure testing the synthesis tower after catalyst loading. Some plants do not have nitrogen or only have low-pressure nitrogen; for pressure testing of medium-pressure or high-pressure synthesis towers, syngas (a mixture of hydrogen and nitrogen) is used directly. This resulted in the catalyst overheating.
Reply #6 2017-03-28
The catalyst manufacturer doesn’t allow you to use high-pressure hydrogen and nitrogen, nor does it permit the use of air; you need to figure out what to do on your own
Reply #7 2017-03-28
Low-pressure methanol catalysts are at risk of excessive temperature rise when operating under a hydrogen-nitrogen gas mixture ratio of 3:1 at a pressure of 1.5 MPa.
Reply #8 2017-03-29
I’m not sure whether you want to perform pressure testing for leaks in the synthesis tower, or to conduct pressure resistance testing on the catalyst that has been loaded

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