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Wastewater analysis

2020-12-16View Original

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In chromatography, what exactly is the procedure for purge and headspace analysis?
Reply #22020-12-16
You had better read professional books on gas chromatography. Purging generally refers to a specific operation in which a carrier gas is used to clean the column system, removing any residues of previous analytes that might remain in it, so as not to affect subsequent analyses. Headspace analysis, as the name implies, involves analyzing the gaseous components present in the space above a liquid; it is typically used for analyzing highly volatile compounds, unlike methods in which the sample is directly introduced into the analysis column system through a sampling valve or injector. This method is often used for sampling VOC analysis in water, but headspace sampling requires control of certain conditions, such as temperature and the equilibrium time of the sample in the gas phase. It’s not a very accurate explanation; it’s just for reference.
Reply #32020-12-16
Thank you for the answer; I get it roughly! I will learn the *related theories again, and then learn the *operations.
Reply #42020-12-16
You had better read professional books on gas chromatography. Purging generally refers to a specific operation in which a carrier gas is used to clean the column system, removing any residues of previous analytes that might remain in it, so as not to affect subsequent analyses. Headspace analysis, as the name implies, involves analyzing the gaseous components present in the space above a liquid; it is typically used for analyzing highly volatile compounds, unlike methods in which the sample is directly introduced into the analysis column system through a sampling valve or injector. This method is often used for sampling VOC analysis in water, but headspace sampling requires control of certain conditions, such as temperature and the equilibrium time of the sample in the gas phase. It’s not a very accurate explanation; it’s just for reference.

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