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How to remove pyridine mixed in chloroform?

2007-12-23View Original

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Our company does not have distillation towers. The mother liquor contains chloroform and pyridine; in the past it was possible to separate chloroform from pyridine, but this time the chloroform contains about 1% pyridine, and re-distillation cannot remove this compound. Water washing also has little effect – what should we do?
Reply #22007-12-23
Chloroform has a boiling point of 64 degrees. What is pyridine? A 1% concentration doesn’t seem to have much impact, so it shouldn’t be a problem
Reply #32008-02-26
Neutralization with hydrochloric acid is carried out to form a salt of pyridine; subsequent washing and separation by layering ensures the removal of pyridine from chloroform
Reply #42018-05-31
I would like to ask what materials should be used for the tower and pipelines in the distillation of chloroform and pyridine? How is the corrosion?

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