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Problems with product extraction in distillation columns

2008-01-27View Original

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This post was last edited by Black gold on 2011-11-28 at 16:35. The distillation column used in our company operates under negative pressure (–0.1 MPa), and the reflux volume at the top of the column remains around 2 tons. Why isn’t there any side-stream extraction? It is a full-reflux column.
Reply #22008-01-27
What is the diameter of the tower? What is the porosity? There must be a leak; there is no liquid phase on the collection tray, so no material can be collected
Reply #32008-01-28
It is very likely that since the material entering the product distillation column contains only a small amount of light components, these components are not removed from the top of the column; instead, they are concentrated at the top, and once they reach a certain concentration, they are discharged through intermittent venting! (I hope this is helpful to you)
Reply #42008-01-28
Let’s take this question to the process section; what can be discussed here?

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