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Synthesis of several molecular sieve membranes

2008-10-21View Original

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1: In-situ hydrothermal synthesis method: Also known as in-situ hydrothermal crystallization method, this approach involves placing the carrier in the molecular sieve synthesis solution; at a certain temperature, pressure is generated within a crystallization chamber, allowing molecular sieve crystals to form a film on the surface of the carrier. 2: Crystal method: Also known as the secondary growth method, it involves using physical techniques [such as dip-coating, polishing, ultrasonic treatment, etc.] to first form a layer of molecular sieve seeds or film on the surface of the substrate. The carrier is then placed in the molecular sieve synthesis mother liquor and crystallized into a film under certain hydrothermal synthesis conditions. 3: Pore-blocking method: This involves immersing the carrier in a synthetic mother liquor, and then creating a negative pressure through vacuum pumping to allow the mother liquor to enter the pores of the carrier. Under certain hydrothermal synthesis conditions, molecular sieve crystals grow within these pore channels. Since the molecular sieve crystals grow inside the carrier’s pores, the resulting molecular sieve membrane possesses improved mechanical strength and thermal stability. 4: Microwave heating method 5: Pulse laser deposition method 6: Electro-pulsed deposition method. I hope to discuss such technologies with everyone. Thank you for your participation! ! ! !
Reply #22008-10-22
It’s a different type of membrane from what I use; I’ve learned about it. Could someone upstairs explain it in more detail?
Reply #32008-12-01
Could the information be provided in more detail?
Reply #42008-12-02
As for how to prepare molecular sieve seeds, I would like to ask everyone: should one simply take a certain amount of molecular sieve and add water to it, or should molecular sieve synthesis solution be used?
Reply #52008-12-03
I’ve learned it; it’s great knowledge~~~~
Reply #62010-06-28
Reply to 4# *aoshanxn: Both methods work; I’m working on this right now
Reply #72010-06-28
Reply to 7# lxhgy411: Get in touch with me; I have a fairly complete collection of this material
Reply #82010-06-28
Recently, I have been working a lot on using microwave heating to prepare continuous and thin molecular sieve membranes. At present, I am still using the secondary growth method for this purpose; I haven’t explored the use of microwaves yet
Reply #92010-06-28
I’ve learned *a bit more knowledge! Thank you

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