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How to collect samples

2009-02-02View Original

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How to collect samples; Gasoline, diesel, slurry, crude oil, benzene, ethylene, propylene, dry gas, nitrogen, etc. Who can help me solve it? grateful! This post was last edited by bingyu252 on 2009-2-2 13:06 ]
Reply #22009-02-02
Liquids should have dedicated sampling valves. Not easy to generate static electricity. High-temperature oil products have cooling devices. Before sampling, check whether there are any unsafe factors such as fire sources in the surrounding area. The sampling flow rate should be slow. The sampling container complies with safety regulations. To collect gas samples, a special sampler is required. For details, please refer to the "Petroleum Liquid Manual Sampling Method." In recent years, many static electricity ignition accidents have occurred during the oil sampling process in oil tank areas. Although they did not cause large economic losses, they still had an adverse impact on the normal production of enterprises. The risk of static electricity in sampling mainly comes from unqualified sampling equipment and improper operation. 1. Standing time "Guidelines" stipulate that large oil tanks should be left standing for 30 minutes after filling with oil before sampling and other operations. Most companies can do this, but some companies still have the phenomenon of dynamic sampling, and the risk of static electricity is greater. 2. Human body static electricity sampling workers should wear anti-static shoes, clothes and gloves, and discharge static electricity from the human body before putting on the can and covering the sampling port. 3. The sampling equipment used by most enterprises is qualified. Plastic buckets tend to accumulate static electricity during movement. Some companies use them to hold sampling equipment and lift them to the top of the tank, which is very dangerous. 4. Sampling rope Most enterprise operators do not reliably ground the sampling rope during the sampling process. Since the sampling rope is valid within 3 months, most of them failed to pass the actual test.
Reply #32009-02-02
GB/T 6678-2003 General principles for sampling of chemical products GB/T 3723 General principles for sampling safety of industrial chemical products (GB/T 3723-1999, idt ISO 3165:1976) GB/T 6679 General principles for sampling of solid chemical products GB/T 668. General rules for sampling of liquid chemical products GB/T 6681 General rules for sampling of gas chemical products
Reply #42013-11-26
A professional tank automatic sampling device manufacturer with leading principles, performance and quality--Beijing Century Kaituo Equipment and Instrument Co., Ltd. 010-57018538 57263297 E-mail: chemtool@126.com , the sampling device produced by our company adopts a proportionally telescopic stainless steel pipe truss structure, and controls the stress state of the truss in the oil to a nearly weightless state, so that the entire truss rises and falls in proportion to the liquid level, ensuring that the sampling points on it change in proportion and meet the sampling point division requirements stipulated in the "Petroleum Liquid Manual Sampling Law" at all times. A highly integrated modular operation box is used outside the tank, and 3 special valves (samplers from other manufacturers are usually equipped with no less than 7-12 valves) solve all the functions of a. emergency cut-off function, b. sampling selection switching, c. "dead sample" cycle replacement/sampling. The self-developed circulation pump can be used for all oil products (from naphtha to asphalt). The self-developed special two-position multi-way emergency shut-off valve function ensures that any component can be repaired and replaced under normal operation of the tank. The self-developed special sample selection switching valve can be used in any forward or reverse rotation. The special sampling valve ensures that each sample is collected without dead samples. There is also detection equipment to detect whether the oil is flowing when the sampling device is replaced by a cycle. Our company's automatic tank sampling device can simply collect five samples specified by the sampling standards: upper sample (1/6 liquid level below the liquid surface), middle sample (1/2 liquid level below the liquid surface), lower sample (5/6 liquid level below the liquid surface), bottom sample (tank bottom surface), and outlet liquid level sample (corresponding liquid level on the lower edge of the tank output port). It can also set up a quick combined sample (a. upper sample): middle sample: Lower sample=1:1:1 or b. Upper sample: middle sample: Outlet liquid level sample = 1:1:1, combined sample volume error is not greater than 1%). At present, it has been used in most petrochemical enterprises in China, with a total of nearly 2,000 sets. And through continuous technological improvement, the product has reached a maintenance-free quality level.

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