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Purification of acids containing organic impurities

2009-02-11View Original

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The hydrogen bromide produced today contains certain organic impurities (p-tolylformaldehyde), which affects the sales of the product. I tried using tributyl phosphate for extraction; the color of the solution changed from a slight red to a transparent color, but the liquid tended to cling to the walls of the container, not appearing as natural as water. I’m not sure why this happens. I would like to ask experienced seniors for help – how should I get rid of these organic impurities, and what methods can be used? ? ? Can membrane separation be used? Note: The concentration of HBrde produced by our company is 48%; the concentration of p-tolylformaldehyde is unknown, but it is certainly not high, likely below 2%. Distillation in this case would be somewhat counterproductive, as there are very few impurities, and the production volume is quite large – 3-4 tons per day! This post was last edited by Termitic Chief on 2009-2-11 09:44]
Reply #22009-02-11
Push it yourself to keep it from sinking
Reply #32009-02-11
Ultrafiltration, nanofiltration, and reverse osmosis definitely won’t work. It is not yet known whether other membrane separation methods will work.
Reply #42009-02-17
Could everyone give some advice? Looking forward to it

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