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How to address coking issues during the distillation of organic compounds?

2009-02-26View Original

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During the distillation of organic compounds, coking of the coil in the reboiler heater results in insufficient heat transfer capacity of the heat exchanger. How can such problems be solved? Using vacuum distillation may result in the removal of organic substances, affecting the material consumption per unit of product
Reply #22009-02-26
"Coil of the reactor bottom heater” – “It seems you’re using a batch type; you might consider switching to a thermosyphon type.” Increase the cycle time to reduce the residence time on the heating tube
Reply #32009-02-26
Could forced circulation be considered?
Reply #42009-03-12
Thanks to the person above; forced cycling is available now

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