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1. Fill in the blanks: 1. When distilling petroleum products, ( ) must be placed in the distillation flask to prevent bumping. 2. The method of treating mercury-containing waste liquid is: Add -( ) to the waste liquid to form ( )-precipitate. 3. After taking the liquid argon sample, pay attention to keeping the cylinder pressure below ﹙ ﹚Mpa, and always pay attention to the pressure relief to prevent the cylinder from overpressure. 4. When taking cryogenic liquid samples on site, you should cooperate with on-site ( ) personnel to connect the sampling cylinder. 6. When taking ( ) samples of boiler water, wastewater, etc., analysts in the water vapor position must wear protective gloves and ( ) open the valve to avoid burns. 7. Do not replace the dynamic fire under pressure, and the maximum oxygen content in the system shall not exceed ( )%. 8. When safely entering for analysis, the oxygen content is within ( )% to be qualified. 9. There are four common methods of artificial respiration: ( ), ( ), ( ), and ( ). 10. Harmful factors in the production environment include ( ), ( ), ( ). 2. Judgment 1. After the oil analysis is completed, the remaining samples cannot be poured into the sewer and must be recycled centrally. ( ) 2. The sample can be dissolved with aqua regia in a platinum crucible. ( ) 3. Methanol is an irritating poison ( ) 4. N2 is an asphyxiating poison ﹙ ﹚ 5. When handling the double platinum wire electrode of the DL35 moisture meter, the electrode can be cleaned in an ultrasonic bath of deionized water or ethanol for a few minutes, or soaked in chromic acid wash solution for 60 seconds, and then rinsed with water or ethanol and fully dried. ( ) 7. When using the DFY-IVB oxygen analyzer for pipe network replacement analysis or gasifier feeding analysis, the oxygen injection flow rate is controlled to 600ml/min. ( ) 8. The gasifier is now feeding, and a sample is retrieved and analyzed with the DFY-IVB oxygen analyzer. If the screen number continues to decrease and displays zero, the reported data indicates that the oxygen content has not been detected. ( ) 9. Dangerous chemicals refer to chemicals that are explosives, compressed gases and liquefied gases, flammable liquids, flammable solids, self-igniting items and flammable items when wet, oxidants and organic peroxides, toxic drugs and corrosives. ( ) 10. Hazardous chemical accidents refer to personal casualties, property losses or environmental pollution accidents caused by the accidental release of one or several hazardous chemicals or their energy. ( ) 3. Questions and Answers: 1. What should you pay attention to when taking concentrated acid and concentrated alkali samples? 2. Briefly describe how to safely handle liquid oxygen residual liquid. 4. * * What is the allowable concentration of toxic and harmful gases? 5. How to use filter gas mask? This post was last edited by Cang Hai Yisha on 2009-4-8 15:56 ]
1. 1. Zeolite 2. Sodium sulfide, mercury sulfide 3. 4.0 4. Process operation 6. High temperature; Slow 7,0. 5 8. 18-20.9 9. Supine chest press pose ; prone position ; Supine arm pose ; Mouth-to-mouth, mouth-to-nose type 10. Physical factors ; chemical factors ; Biological factors 2, 1, True 2, False 3, False 4, True 5, True 7, False 8, False 9, True 10, True 3, 1, Answer: (1) Wear protective equipment correctly, including at least protective glasses, acid and alkali resistant overalls, and acid and alkali resistant gloves. (2) Try to use large-mouthed sampling vessels. (3) If you accidentally splash concentrated acid or alkali on your skin, rinse with plenty of water for more than 15 minutes. 2. Answer: Liquid oxygen residual liquid must not be dumped in the instrument room to prevent injury to people, and to prevent large amounts of liquid oxygen from evaporating and causing excessive local oxygen concentration, causing unsafe accidents. 4. Answer: Methanol (steam) ≤50mg/m3 Carbon monoxide ≤30mg/m3 Ammonia ≤30mg/m3 Hydrogen sulfide ≤10mg/m3 Dimethyl ether ≤400ppm 5. Answer: 1) Connect the mask to the airway filter tank in the order of the mask and trachea filter. 2) Check whether the mask is airtight and intact. Then open the bottom plug. 3) Put the filter tank into the mask bag, fasten the bag cover, then carry the mask on your left ribs and right shoulders, and fasten the belt. 4) Put on the mask as you would wear a mask, and take a few breaths to prove that there is no problem with the mask before entering the poisonous area.
1. Fill in the blanks 1. There are two commonly used methods for decomposing samples ( ), ( ). 2. When measuring the viscosity of an oil sample, ( ) must be removed first, because impurities will affect the flow of the sample in the viscometer. 3. The "Hygienic Standards for Design of Industrial Enterprises" stipulates that the maximum allowable concentration of ammonia in the air in the production environment is ﹙ ﹚ mg/m3 4. After taking the liquid carbon dioxide sample, you should open the ﹙ ﹚ slightly to exclude some samples to keep the cylinder pressure from being too high. Make sure the sample is safe and then close the valve. 7. Safety analysis includes ( ) and ( ). 8. If methanol liquid accidentally enters the eyes or enters the mouth by mistake, rinse immediately with ( ), gastric lavage and induce vomiting and sent to the hospital. 9. The symptoms of poisoning are divided into ( ), ( ), ( ). 10. Cardiac resuscitation can be applied at the scene ( ), ( ). 2. True or False Questions 1. The correct procedure for distillation operation is to turn on the heating equipment first and then turn on the condensation water. At the end, turn off the heating equipment first and then turn off the condensation water. ( ) 2. The waste liquid discharged when measuring chloride ions by mercury measurement method is poured directly into the sewer. ( ) 3. The "Hygienic Standards for Design of Industrial Enterprises" stipulates that the maximum allowable concentration of methanol in the production environment air is 50 mg/m3﹙) 4. Argon is not a highly toxic gas﹙﹚ 5. When using microwave digestion to process samples, any organic reagents and volatile substances can be directly digested. ( ) 6. When measuring dissolved oxygen in boiler feed water, the water sample after color development is very alkaline, so contact with skin should be avoided as much as possible. After each test, hands should be rinsed immediately with clean water to avoid eroding the skin. ( ) 7. When safely entering the tank for analysis, take the middle and upper gas sample when the density of the gas to be measured is greater than the density of air. ; When the density is less than the air density, take the middle and lower air samples. 8. Samples for safe entry analysis and Class I fires should be retained for half an hour, and samples for special fires should be retained until the end of the fire. 9. Filter gas masks are strictly prohibited from being used for all kinds of asphyxiating gases. ( ) 10. Dangerous targets refer to places or facilities where hazardous chemicals may cause accidents due to their dangerous nature and quantity. ( ) 3. Questions and Answers 1. How to deal with hydrofluoric acid burns? 2. Briefly describe the safety precautions when sampling liquid argon. 3. Briefly describe urea’s main tendency to block sample points and the precautions to be taken when clearing pipelines. 4. What are the safety precautions for the gas chromatograph analysis room? 5. What does fire protection facilities include?
1. 1. Dissolution method, melting method 2. Mechanical impurities 3., 30 4. Liquid phase valve (black side) 7. Dynamic fire analysis; Safety entry analysis 8. 2% sodium bicarbonate 9. Mild poisoning ; Moderate poisoning ; Severe Poisoning 10. Precardial Tapping Technique ; Chest compression surgery 2, 1, False 2, False 3, True 4, True 5, False 6, True 7, False 8, True 9, True 10, True 3, 1, Answer: Hydrofluoric acid burns can corrode not only skin, tissue, and organs, but also bones. Wear protective gloves and safety glasses when working with hydrofluoric acid, and do so in a fume hood. In case of accidental contact with the skin, rinse immediately with plenty of water, and then apply mercurochrome or freshly prepared 20% MgO glycerin solution to the affected area. Go to the hospital for treatment in severe cases. 2. Answer: ①Two people should go together when taking samples, dress according to regulations, and wear protective gloves to prevent low-temperature burns. ②Connect the sampling cylinder, open the sample valve, and then open the cylinder inlet and outlet valves one after another to fully replace the cylinder with liquid spray. After the replacement is completed, close the cylinder inlet and outlet valves, open the large sample valve and the cylinder inlet valve to take samples. After the outside of the cylinder is frosted, first close the cylinder inlet valve, then close the main valve of the sample pipeline, and then remove the connection. ③After taking the liquid argon sample, pay attention to keeping the cylinder pressure below 4.0Mpa, and always pay attention to the pressure relief to prevent the cylinder from being overpressured. ④ When taking samples, use stainless steel tubes to connect to the instrument to ensure the air path is sealed, and adjust the flow rate to prevent damage to the instrument. 3. Answer: 1) Most urine samples are prone to clogging when the ambient temperature is low and require steam purging. The main sample points are S-201, S-202, S-402, S-102, and S-103. 2) When using steam, hold the hose with one hand or step on the hose with your feet, and then slowly open the steam valve to prevent the steam hose from swinging and injuring people. 4. Answer: Regularly check the joints and connections of the carrier gas pipeline for air leakage. Regularly check that chromatographs equipped with FID detectors are not extinguished, causing hydrogen to be released into the environment. Check the power supply regularly to see if there is any leakage or aging that could cause a fire. Pay attention to the ventilation effect of the laboratory to avoid causing low indoor oxygen content or hydrogen accumulation. 5. Answer : 1) Fire station 2) Fire water supply facilities: Fire water supply pipes and fire hydrants. 3) Fire water supply facilities in chemical production equipment areas: Fire water supply supervision, cooling sprinkler system, fire water mist, and water cannon.
1. Fill in the blanks 1. The main substances causing pollution in chemical production are ( ), ( ), ( ), ( ). 2. The circuit is composed of four parts ( ), ( ), ( ), ( ). 3. The hazards that industrial dust can cause include carcinogenesis, poisoning, pneumoconiosis and skin (). 4. Liquid ammonia splashed into the eyes can cause redness and swelling of the conjunctiva, cornea ( ), and even blindness. 7. An existing safety inlet analysis found that the carbon monoxide content was 100ppm, converted to ( ) mg/m3. 8. The boiling point of dimethyl ether is ( ) degree. When sampling products, use ( ) to carry the sample. 9. The ways in which industrial poisons invade the human body ( ), ( ) ( ). 10. Gases are divided into ( ), ( ), ( ), ( ), ( ), ( ) gases according to their toxic effects. 2. True or False Questions 1. When measuring the opening flash point of an oil sample, spontaneous combustion may sometimes occur, and the fire must be extinguished with water. ( ) 2. When turning on a computer-controlled analytical instrument, in order to ensure the safety of the instrument, the correct startup sequence should be to turn on the host first, and then turn on external devices such as printers and monitors. ( ) 3. When ammonia splashes into the eyes, the first aid measure that should be taken immediately is to send to the hospital ﹙ ﹚ 4. The first aid measure for accidentally ingesting methanol is gastric lavage ﹙ ﹚ 5. Do not use dehydrating solvents (such as K2Cr2O7 lotion, absolute ethanol and concentrated H2SO4, etc.) to clean the glass electrode to prevent damage to the performance of the electrode. ( ) 6. All Karl Fischer reagents are highly flammable solutions and are toxic. Do not inhale or swallow. Avoid contact with skin. ( ) 7. There is a gas sample with an oxygen content of (30-35)%, and the AIM-450 oxygen detection alarm instrument is used for analysis. ( ) 8. When sampling inside the equipment, the sampling depth should be greater than 2 meters. ( ) 9. Poisons used or produced in industrial production are called industrial poisons. ( ) 10. Falsely reporting a fire alarm is not an act that disturbs public order. ( ) 3. Questions and Answers 1. What should you pay attention to when using strong acid? : 4. What precautions should be taken when using high-pressure cylinders? 5. What are the general principles of fire fighting?
1. 1. Heavy metals, acid-base pollutants, organic pollutants, solid pollutants 2. Power supply, wires, switches, loads 3. Inflammation 4. Ulcer 7. 125 8. -24.9; Cylinder 9. Respiratory tract, digestive tract, skin and mucous membranes 10. Irritation, suffocation, * * Sex, pyrogenicity, corrosivity, sensitization 2. 1. False 2. False 3. False 4. False 5. True 6. True 7. False 8. True 9. True 10. False 3. 1. What should you pay attention to when using strong acids? answer: (1) Rubber gloves should be worn when using strong acids ; (2) Glass products such as measuring cylinders are required when measuring strong acid. (3) When diluting strong acid, be sure to slowly pour the concentrated acid into the water along the wall of the container and stir while pouring. Never pour water into the strong acid. 4. What precautions should be taken when using high-pressure cylinders? answer: 1) High-pressure gas bottles must be stored in categories and labeled according to gas type. 2) Store gas cylinders in a cool, dry place. Keep open flames away from heat sources and prevent exposure to the sun. 3) Handle the gas cylinder with care and do not knock it or shake it violently. The bottle body has two anti-shock rubber rings. It is strictly forbidden to roll the acetylene bottle horizontally. Gas cylinders should undergo regular technical inspections and pressure tests. 4) The pressure reducing valve for high-pressure gas cylinders should be dedicated. Oxygen and hydrogen pressure reducing valves should be distinguished, and there should be no air leakage at each connection. 5)|The gas in the bottle must not be completely exhausted, and a residual pressure of (0.2-1.0) MPa should be maintained to prevent danger. Hydrogen bottles and oxygen bottles must not be stacked close to each other to prevent danger. 6) This sample point is easily blocked and is equipped with a steam purge pipeline. It must be operated in order. 5. What are the general principles of fire fighting? answer: 1) If you call the police early, the loss will be less, and you can call the police and put out the fire at the same time. 2) Control first, then put out the fire, save people first, then save things. 3) If there is room poisoning, prevent suffocation, listen to instructions and don’t panic.