About acidolysis and alkaline hydrolysis of dibromide
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Now we have a product that generates aldehyde through the acidolysis of dibromide. Because dibromide contains tribromide, the by-product acid is generated after acidolysis.； Now I want to suppress or remove the by-product acid, and I want to use alkali washing method to alkaline decompose dibromide in alkali to generate -aldehyde. The method of acidolysis is very mature, but I don't know much about the alkaline hydrolysis of dibromide. I have done experiments on alkaline deacidification of the products after acidolysis of dibromide, and the results are very few. I would like to ask if any of you have experience in the alkaline hydrolysis of dibromide or dichloride to form aldehydes! Please advise! How should it be done?
If there are trihaloalkyl, alkaline hydrolysis will not produce aldehydes. When the acid generated by acid hydrolysis is removed with alkali, the alkali concentration should have a great influence, because aldehydes are unstable under alkaline conditions, so I think if you adjust the alkali concentration, it should be no problem! !
I just use 5% NaOH, alkaline solution. It took a long time, so almost nothing precipitated! depressed
You should have Na2CO3