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Books on chemical analysis exams

2009-08-01View Original

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This post was last edited by fengxuemei on 2009-8-1 at 13:43. Please recommend a book for the chemical analysis exam; I’m aiming to obtain a certificate, and it would be best if it comes from an authoritative source. Thank you
Reply #22009-08-01
Table of Contents of “Reference Book for Chemical Analysis Exams”
Part I: Introduction
1. Overview
2. Key Points of Knowledge
3. Study Guidelines
4. Basic Exercises

Part II: Titrimetric Analysis
1. Overview
2. Key Points of Knowledge
3. Study Guidelines
4. Basic Exercises

Part III: Acid-Base Titration
1. Overview
2. Key Points of Knowledge
3. Study Guidelines
4. Basic Exercises

Part IV: Precipitation Titration
1. Overview
2. Key Points of Knowledge
3. Study Guidelines
4. Basic Exercises

Part V: Complexometric Titration
1. Overview
2. Key Points of Knowledge
3. Study Guidelines
4. Basic Exercises

Part VI: Redox Titration
1. Overview
2. Key Points of Knowledge
3. Study Guidelines
4. Basic Exercises

Part VII: Gravimetric Analysis
1. Overview
2. Key Points of Knowledge
3. Study Guidelines
4. Basic Exercises

Part VIII: Colorimetric and Spectrophotometric Analysis
1. Overview
2. Key Points of Knowledge
3. Study Guidelines
4. Basic Exercises

Part IX: Gas Chromatography
1. Overview
2. Key Points of Knowledge
3. Study Guidelines
Reply #32009-08-01
What specific certification in chemical analysis does LZ want to obtain? Is it a certificate for engineers or for laboratory technicians? There is a lot of information on the forum regarding laboratory technician exams, including those for beginners, intermediates, and advanced levels. You can use the “search” function to find it.
Reply #42009-08-01
Table of Contents of Practical Handbook for Laboratory Technicians
Chapter 1: The Laboratory
Section 1: Role of Analytical Testing and Classification of Methods
Section 2: Basic Requirements for a Laboratory
Section 3: Common Glass Instruments and Quartz Products Used in Laboratories
Section 4: Non-glass Containers Used in Laboratories
Section 5: Common Electrical Equipment in Laboratories
Section 6: Management of Laboratory Supplies and Instruments
Section 7: Balances
Section 8: Computing Instruments – Electronic Calculators
Section 9: Water for Laboratory Use
Section 10: Chemical Reagents
Section 11: Laboratory Safety
Section 12: Common Desiccants and Absorbents in Laboratories
Section 13: Common Refrigerants and Adhesives in Laboratories
Section 14: Masking Agents and Unmasking Agents
Section 15: Organic Solvents and Surfactants

Chapter 2: Units of Measurement and Basic Constants
Section 1: Units of Measurement
Section 2: Basic Constants

Chapter 3: Physical and Chemical Properties of Common Compounds
Section 1: Physical and Chemical Constants of Inorganic Compounds
Section 2: Physical and Chemical Constants of Organic Compounds
Section 3: Others

Chapter 4: Solutions and Their Preparation Methods
Section 1: Common Units of Measurement Used in Solution Preparation
Section 2: Methods of Expressing Solution Concentration and Its Calculation
Section 3: Preparation of Common Solutions

Chapter 5: Errors, Significant Figures, Data Processing, and Quality Assurance in Analytical Testing
Section 1: Errors
Section 2: Significant Figures
Section 3: Data Processing
Section 4: Quality Assurance in Analytical Testing

Chapter 6: Standard Methods and Reference Materials
Section 1: Standardization and Standards
Section 2: Standard Methods
Section 3: Standard Methods for Analysis and Testing Published in China
Section 4: Reference Materials
Section 5: Some Reference Materials in Use in China
Section 6: Common Standard Solutions Used in Analysis and Their Preparation

Chapter 7: Qualitative Analysis and Determination of Physical Constants
Section 1: Qualitative Analysis of Inorganic Substances
Section 2: Qualitative Analysis of Organic Substances
Section 3: Methods for Determining Physical Constants

Chapter 8: Quantitative Analysis Process
Section 1: Sampling, Preparation, and Storage of Samples
Section 2: Sample Decomposition – Sample Treatment Before Analysis of Inorganic Substances
Section 3: Elimination of Interferences
Section 4: Determination of the Content of Components to Be Measured in Samples
Section 5: Calculation of Quantitative Analysis Results

Chapter 9: Common Separation and Purification Methods
Section 1: Recrystallization and Sublimation
Section 2: Precipitation Separation
Section 3: Evaporation and Distillation
Section 4: Extraction Separation

Chapter 10: Titrimetric Analysis
Section 1: Principles of Titrimetric Analysis
Section 2: Calculations in Titrimetric Analysis
Section 3: Basic Operations in Titrimetric Analysis
Section 4: Acid-Base Titration
Section 5: Complexometric Titration
Section 6: Redox Titration
Section 7: Precipitation Titration
Section 8: Fluorimetric Titration
Section 9: Aqueous-Outside Titration

Chapter 11: Mass Spectrometry
Section 1: Principles and Calculations in Mass Spectrometry
Section 2: Basic Operations in Mass Spectrometry
Section 3: Applications of Mass Spectrometry

Chapter 12: Electrochemical Analysis Methods
Section 1: Basic Knowledge of Electrochemistry
Section 2: Potentiometric Analysis
Section 3: Conductivity Analysis
Section 4: Electrolysis and Coulometric Analysis
Section 5: Voltammetric and Polarographic Analysis
Section 6: Stripping Voltammetry

Chapter 13: Colorimetry and Ultraviolet-Visible Spectrophotometry
Section 1: Basic Principles
Section 2: Visual Colorimetry
Section 3: Spectrophotometry
Section 4: Selection of Colorimetric Conditions
Section 5: Role of Spectrophotometry

Chapter 14: Fluorimetric Analysis
Section 1: Basic Principles of Fluorimetric Analysis
Section 2: Fluorimetric Spectrophotometers
Section 3: Applications of Fluorimetric Analysis

Chapter 15: Infrared Spectroscopy Analysis
Section 1: Basic Theory
Section 2: Infrared Spectrophotometers
Section 3: Characteristic Absorption Bands and Group Frequencies of Organic Substances
Section 4: Sample Preparation
Section 5: Applications of Infrared Spectroscopy

Chapter 16: Atomic Emission Spectroscopy Analysis
Section 1: Atomic Spectra
Section 2: Prism Spectrometers and Grating Spectrometers
Section 3: Qualitative and Semi-quantitative Analysis Methods for Emission Spectra
Section 4: Quantitative Analysis Methods for Emission Spectra
Section 5: Inductively Coupled Plasma Emission Spectroscopy

Chapter 17: Atomic Absorption Spectroscopy Analysis
Section 1: Basic Principles
Section 2: Atomic Absorption Spectrophotometers
Section 3: Selection of Experimental Conditions and Elimination of Interferences
Section 4: Analysis Techniques in Atomic Absorption Spectroscopy
Section 5: Applications of Atomic Absorption Spectroscopy
Section 6: Atomic Fluorescence Spectroscopy

Chapter 18: Chromatography Analysis
Section 1: Column Chromatography
Section 2: Paper Chromatography
Section 3: Thin-Layer Chromatography
Section 4: Paper Electrophoresis

Chapter 19: Gas Chromatography
Section 1: Introduction to Gas Chromatography
Section 2: Gas Chromatographs
Section 3: Fixed Phases in Gas Chromatography
Section 4: Common Detectors in Gas Chromatography
Section 5: Qualitative Analysis in Gas Chromatography
Section 6: Quantitative Analysis in Gas Chromatography
Section 7: Inspection and Troubleshooting of Common Faults in Gas Chromatography
Section 8: Applications of Gas Chromatography

Chapter 20: High-Performance Liquid Chromatography
Section 1: Basic Theory
Section 2: Process and Equipment
Section 3: Types and Applications
Section 4: Derivatization Techniques, Qualitative, Quantitative, and Applications

Chapter 21: Application of Microcomputers in Analytical Chemistry
Section 1: Computers and Analytical Instruments
Section 2: Internal Structure of Microcomputers
Section 3: External Devices of Computers and Analytical Instruments
Section 4: Software Systems of Microcomputers
Section 5: Common Chinese Character Processing Systems for Microcomputers
Section 6: Examples of the Application of Microcomputers in Analytical Instruments

Chapter 22: Analytical Chemistry Literature and Its Retrieval
Section 1: Overview of Scientific Literature Retrieval
Section 2: Analytical Chemistry Literature and Retrieval Tools
Section 3: Standard Literature
Section 4: Methods of Searching for Literature

Chapter 23: Writing of Scientific Documents
Section 1: Overview of Scientific Documents
Section 2: Writing of Scientific Reports and Papers
Reply #52009-08-01
The original poster didn’t explain it clearly! ~There is a difference between chemical analysis, industrial analysis, and being a laboratory technician! ~
Reply #62009-08-05
Chemical Analysis http://img1.chem17.com/3/20090121/633681461266618750.jpg Chapter 1 Basic Knowledge of Chemical Analysis 1 Section 1 Tasks and Methods of Chemical Analysis 1 1. Tasks and Roles of Chemical Analysis 1 2. Methods of Quantitative Analysis 1 Section 2 Errors and Analysis of Data Processing 3 1. Errors in Quantitative Analysis 3 2. Representation of Analysis Results 6 3. Data Recording and Experimental Reports 11 4. Regression Analysis 12 Section 3 Preparation of General Solutions 13 1. Chemical Reagents 13 2. Laboratory Water 15 3. Preparation of Auxiliary Reagent Solutions 16 4. Preparation of Common Laboratory Detergents 18 Section 4 Laboratory Safety Knowledge 19 1. Laboratory Safety Rules 19 2. Handling and Prevention of Laboratory Accidents 19 3. Disposal of Laboratory Waste 22 Thought Questions and *Questions 23 Chapter 2 Basic Operational Techniques in Chemical Analysis 27 Section 1 Balances and Their Use 27 1. Tray Balances 27 2. Analytical Balances 28 3. Methods for Weighing Samples 33 Section 2 Glass Instruments and Other Equipment 33 1. Common Glass Instruments 34 2. Other Common Equipment 37 3. Common Measuring Instruments 38 Section 3 Sampling and Sample Processing 40 1. Principles of Sampling 40 2. Sampling of Liquid Samples 40 3. Sampling of Gas Samples 41 4. Sampling and Preparation of Solid Samples 42 Section 4 Basic Operations in Titrimetric Analysis 43 1. Use of Droppers 43 2. Use of Volumetric Flasks 46 3. Use of Pipettes 47 4. Calibration of Volumetric Instruments 49 Experiment 1 Practice in Weighing with an Analytical Balance *52 Experiment 2 Basic Operations of Titrimetric Analysis Instruments 54 Experiment 3 Calibration of Titrimetric Analysis Instruments 56 Thought Questions and *Questions 57 Chapter 3 Quality Assurance and Standardization in Chemical Products 60 Section 1 Quality Assurance in Chemical Analysis 60 1. Quality Control in Chemical Analysis 60 2. Quality Evaluation in Chemical Analysis 61 Section 2 Standardization and Standards 61 1. Meaning of Standardization 61 2. Basic Knowledge of Standards 62 3. Adoption of International and Advanced Foreign Standards 65 Thought Questions and *Questions 67 Chapter 4 Titrimetric Analysis 69 Section 1 Conditions and Methods of Titrimetric Analysis 69 1. Basic Conditions for Titrimetric Analysis 69 2. Methods of Titrimetric Analysis 69 Section 2 Standard Titrant Solutions 70 1. Methods of Expressing the Concentration of Standard Titrant Solutions 70 2. Preparation and Calibration of Standard Titrant Solutions 71 Section 3 Basic Calculations in Titrimetric Analysis 72 1. Rules for Equimolar Reactions 72 2. Calculations for Adjusting the Concentration of Standard Solutions 73 3. Examples of Calculations 74 Thought Questions and *Questions 76 Chapter 5 Acid-Base Titration Method 79 Section 1 Introduction to the Method 79 1. Acid-Base Proton Theory 79 2. Calculation of pH in Acid-Base Aqueous Solutions 80 3. Buffer Solutions 82 Section 2 Acid-Base Indicators 85 1. Principle of Color Change and Color Range of Indicators 85 2. Common Acid-Base Indicators 87 Section 3 Titration Curves and Selection of Indicators 88 1. Titration of Strong Acids or Bases 88 2. Titration of Weak Acids or Bases 90 3. Titration of Polyacids and Polyacid Salts 92 Section 4 Modes and Applications of Acid-Base Titration 94 1. Direct Titration 94 2. Back Titration 96 3. Indirect Titration 96 Experiment 4 Preparation of a Standard Sodium Hydroxide Titrant Solution 97 Experiment 5 Determination of Sulfuric Acid Content in Industrial Sulfuric Acid 99 Experiment 6 Determination of Total Acid Content in Vinegar 100 Experiment 7 Preparation of a Standard Hydrochloric Acid Titrant Solution 101 Experiment 8 Determination of Mixed Bases 103 Experiment 9 Analysis of Industrial Formaldehyde Content 104 Experiment 10 Determination of Ammonium Nitrogen Content in Fertilizers 106 Experiment 11 Analysis of Ammonia Content in Ammonia Water 107 Thought Questions and *Questions 109 Chapter 6 Complexometric Titration Method 111 Section 1 Overview 111 1. Characteristics of Complexometric Titration Method 111 2. Stability Constants of Complex Compounds 112 Section 2 Influence of Acidity on Complexometric Titration 113 1. Forms of EDTA Present 113 2. Influence of Acidity on Complexometric Titration 114 Section 3 Metal Indicators 116 1. Principle of Action of Metal Indicators 116 2. Common Metal Indicators 116 Section 4 Modes and Applications of Complexometric Titration 119 1. Determination of the Content of a Single Component 119 2. Determination of the Content of Multiple Components 120 Experiment 12 Preparation of a Standard EDTA Titrant Solution 122 Experiment 13 Determination of Total Calcium and Magnesium Content in Industrial Water 123 Experiment 14 Sequential Titration of Fe3+ and Al3+ 125 Thought Questions and *Questions 127 Chapter 7 Precipitation Titration and Gravimetric Analysis Methods 130 Section 1 Overview 130 1. Principle of Solubility Product 130 2. Stepwise Precipitation 131 3. Transformation of Precipitates 131 4. Adsorption of Precipitates 131 5. Conditions for Complete Precipitation 132 6. Selection of Precipitating Agents and Sample Quantities 133 Section 2 Precipitation Titration Method 135
Reply #72009-08-15
There is a lot of content like this. The key is to apply what you have learned; it’s not enough to just obtain a certificate.
Reply #82009-08-15
You just need to go to the labor bureau there and ask

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