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Problems with methanol distillation

2010-06-28View Original

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During production, the moisture content of the pure methanol product obtained is above the specified limit; how should this be adjusted? Could that expert please provide a detailed explanation?
Reply #22010-06-28
Common adjustment methods include increasing the top pressure, raising the reflux ratio, and lowering the top temperature
Reply #32010-06-28
The reason for the excessive moisture content in the recovered pure methanol is A: the reflux ratio is too low, causing the heavier components to rise; B. Excessive steam consumption, resulting in too high a temperature at the bottom of the tower ; The adjustment method adopted is A: increase the reflux ratio and reduce the recovery rate ; B. Reduce steam consumption and lower the bottom temperature of the tower

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