Operations in the oxime formation reaction
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The solvent was vacuum-dried, then dissolved in 15 mL of distilled water. The pH was adjusted to 2.0 using 1 mol/L HCl, resulting in the formation of a white precipitate. Dissolve the precipitate in 15 mL of ethyl acetate. How exactly is this operation carried out? Is it necessary to centrifuge the precipitate and then dissolve it in ethyl acetate?
Reply to 1# viger1744125: Is this also an oxime formation reaction? I use hydroxylamine mainly for the oxime formation reaction; why don’t you have it?