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Distillation operation problems

2010-12-13View Original

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In the operation of a distillation tower, how can temperature fluctuations within the tower be avoided?
Reply #22010-12-13
This post was last edited by Chemical Gas Purification on 2010-12-14 08:39. Generally speaking, the temperature inside the tower should remain relatively stable. However, what I’m experiencing is difficult to explain: with no changes in the conditions of feed, product withdrawal, steam, or circulating water, neither the temperature at the top of the tower nor the temperature in the reactor changes, but the intermediate temperature keeps fluctuating. What’s going on? I would appreciate everyone’s guidance. Thank you!
Reply #32010-12-14
It may be related to the composition or properties of your raw materials.
Reply #42010-12-14
The last edit to this post was made by 654262293 on 2010-12-15 at 13:07. Reply 3# jingsan: If it’s a packed tower, it’s possible that the packing has become fouled, resulting in uneven mass and heat transfer between the liquid and gas phases. If it’s a tray tower, there might be a problem with the gas valves
Reply #52010-12-15
Generally, the temperature in the middle of the tower remains stable; such fluctuations are probably due to the filler not being installed properly in that area or something similar
Reply #62010-12-16
I don’t know if there is a condenser at the top of the tower; if so, the problem might lie with the condenser

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