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Before a chemical plant is put into trial operation or full operation, the laboratory needs to carry out many related tasks, such as chromatography calibration and analyzer verification. Who has relevant programs or materials? I would like to learn about them*.
Reply to 1# Cute Doudou: The following are my own opinions; you can take them as a reference :) You could go into more detail. Hehe, if you plan to do these things only before the test drive, it’s probably too late by then. Hehe, at least all the necessary preparations should be done before the test drive. Chromatography calibration should initially be the responsibility of the chromatography manufacturer. During this calibration process, the manufacturer can also provide training to the analysts on how to use the chromatography system. If you already have established analysis conditions, you can ask the manufacturer to carry out the calibration for you. If not, you can figure it out on your own based on the relevant reference criteria. Finally, the samples with known concentrations can be analyzed and compared. Do you mean the factory’s acceptance report for the instrument by the inspection procedure? 1. When a standard instrument arrives at the factory, after the manufacturer unboxes it, the factory staff will be present to count and check all the accessories, spare parts, and other items that come with the instrument. 2. After this checking, it is necessary to verify that the required conditions for water, electricity, etc. are met, including voltage, water quality, gas purity, etc. (the specific requirements depend on the instrument); other infrastructure conditions may also need to be checked. 3. The instrument is then calibrated, and the staff receive training, during which they are informed of the precautions and other relevant information regarding its use. And fill in the manufacturer’s acceptance report (which verifies the condition of the instrument based on the commissioning process); commissioning data is usually included as well. Filling out warranty cards and the like may involve contracts. 4. Once the instrument is ready for use, the factory will, based on its own requirements for the instrument, conduct an inspection and verification using the factory acceptance report (which covers various aspects such as the instrument’s conditions, usage status, data accuracy, and more). The manufacturer’s commissioning and acceptance report + the factory’s acceptance form – these can be signed and certified in the presence of both parties, with copies kept as records. Just keep the contract, warranty card, manufacturer’s phone number, and inspection documents
Main tasks that the laboratory should carry out before starting operations: 1. Determine the instruments required as well as the quality standards for testing raw materials and products in the factory; 2. Please have professional personnel from the manufacturer come to calibrate the instrument; testing facilities should be available ; 3. Master the operation methods of the instruments, and conduct preliminary testing exercises before starting work* ; 4. Purchase reagents and other items required for testing ; 5. Develop testing procedures, and organize examinations and assessments ; 6. Proficient in emergency handling methods for raw materials and products ; 7. Improve various systems.
If it’s a new factory, it will be a bit more troublesome. I think there are several points: First, it is necessary to know which raw materials, semi-finished products, and finished products need to be tested ; Second, testing procedures for each substance must be established ; Third, ensure that all the instruments, equipment, medicines, and reagents needed are available ; Fourth, all personnel have been trained and can likely take up their duties independently ; Fifth is the calibration of instruments and meters.
1. The hardware (including space, equipment, and utilities) is complete, reliable, and ready for use! 2. The job responsibilities are clear ; The staff are well-prepared, with shift arrangements made in accordance with the workload ; 3. Each analysis task requires several practical attempts to ensure that analysis can be carried out immediately upon receipt of the sample ; 4. Prepare emergency plans for potential emergencies! (It’s very important, oh! A brainstorming session can be held to gather everyone’s ideas.) 5. By doing the above things well, you’ll be a great department leader!
First, the personnel need to be in place; second, the standard solutions must be prepared; third, the analysis instruments need to be checked; and finally, timely communication with the production department is necessary. Of course, the various analysis reports must also be prepared