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Analysis method for methanol concentration in methanol aqueous solution?

2011-01-19View Original

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The crude product is purified by recrystallization using methanol as the solvent. The methanol gas and water vapor released during the recrystallization process are condensed in a condenser, resulting in an methanol-water solution with an estimated concentration of around 10–50%. Could you please advise on the method for analyzing the methanol concentration? Thank you!
Reply #22011-01-19
Gas chromatography (with an alcohol column as the chromatographic column) can be used for analysis
Reply #32011-01-20
If chromatography-grade precision is not required, the refractometry method can be considered
Reply #42011-01-20
If online testing is required, an online refractometer can be used; for manual testing, a laboratory refractometer or a portable one can be employed
Reply #52011-12-15
We can help you resolve this issue – it can be installed directly in production without the need for sampling; real-time monitoring is possible, so you might want to take a look
Reply #62012-01-12
Simply put, why use the specific gravity method? It’s so complicated and costly; the specific gravity method is simpler and more practical.

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