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I would like to ask about the separation of cyclohexanol and n-hexanol

2011-03-03View Original

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To separate the n-hexanol from cyclohexanol mixture, it is necessary to reduce the cyclohexanol concentration to below 0.1% (w). Since their relative volatilities are very low, azeotropic distillation or extractive distillation is planned to be used. Does anyone have any good suggestions regarding the choice of extractant or entrainer? I have tried the solvents listed in the solvent manual that are azeotropic with cyclohexanol, but the results were not satisfactory. Also, is there a significant relationship between the azeotrope temperature and temperature? Are there any solvents that are commonly used in extractive distillation? I earnestly hope for your guidance.
Reply #22011-03-05
Why isn’t anyone answering this question? I also hope to see an answer.

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