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Record of Emergency Handling for Slurry Pump Leakage

2011-09-15View Original

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At around 15:20 on April 29, 2010, process personnel at a company’s catalytic unit discovered a leakage at the weld site where the pre-heating line led out from the P208/1 outlet. They immediately reported this to the shift supervisor, who in turn informed the workshop management and production scheduler. Since the leakage amount is small, it can be controlled. The workshop agreed to use emergency plugs to seal the leaks. Contact the processing department to make the clamps. During distillation operations, reduce the frequency of P208/1 appropriately; the shift leader should assign someone to monitor P208 and use steam for shielding. At 15:40, the leakage rate at that point suddenly increased rapidly; the personnel on duty immediately shut down P208/1 and simultaneously notified the fire department and production control team by phone. Significantly reduce the reaction unit’s output (to around 60%) and lower the main air flow, while maintaining normal operations for this unit ; Distillation is used to increase the circulation rates of the re-refined oil returning to the tower (with full closure of the re-refining system), the intermediate oil, and the top-loop oil, as well as the cooling flow rate at the tower top, in order to ensure stable operation and maintain the temperatures at various points. Contact the dispatch to have the unqualified tank changed in the diesel tank area. During the actual control process, proper supervision was provided in the workshop, the operators at their posts acted decisively, the reduction in processing volume was appropriate, the adjustments to the re-refined oil and intermediate top circulation were suitable, the dry point of the crude gasoline met the requirements. After the diesel was separated, the sample analysis showed normal temperatures, so it was transferred back to the qualified tank. Later, the liquid level at the bottom of the tower increased slightly, so the slurry discharge control valve was opened; due to the low viscosity of the slurry, it could be transported to the tank area under its own pressure. After stopping the slurry pump, there is no leakage at the leak point. The Machining Department carried out emergency welding to repair the leakage points. At 17:20, the patch welding was completed. Turn on P208/1; slowly increase the pump outlet pressure – no abnormalities were detected, and operations were gradually resumed. After the clamps were manufactured, the welded areas were reinforced with glue. Production operations have been fully resumed. Thanks to the timely discovery and proper handling of this incident, an accident involving massive leakage and spontaneous ignition was avoided, as well as an emergency shutdown of the facility.
Reply #22011-09-15
Reply: What does 2# yjtlyg mean? It wasn’t explained clearly. Does it mean using modified crude oil to refill the tower for cooling purposes? It was on at first. Later, the level rose and it stopped.
Reply #32011-09-15
From 15:40 to 17:20, an emergency shutdown of P208/1 was carried out, which prevented an emergency stop of the entire plant. Does this mean that the feed was not cut off? I’m not sure what the solid content of the slurry is
Reply #42011-09-15
Reply to 4# Sanlian and Workshop: Yes, of course there’s no material being fed in; otherwise an emergency shutdown would be necessary. But it seems the clasp was made at night.
Reply #52011-09-15
This approach is completely feasible. Once, we encountered a leak in the cross-line valve of the slurry pump; in that case as well, we stopped the slurry pump, increased the flow rate to the maximum in the re-refining tower, and controlled the temperature of the gas phase. We followed this procedure for 5 hours, and after replacing the valve, we increased the slurry circulation rate and the amount of material discharged externally, without the solid content of the slurry exceeding the specified limits. When performing this operation, it is necessary to maintain a stable pressure difference between the two devices in order to prevent catalyst loss.
Reply #62011-09-16
What is the pressure in the distillation tower? Can it be pressurized to the tank area? Additionally, it is recommended that, while under the supervision of designated personnel, fire trucks be stationed on site to ensure emergency preparedness.
Reply #72011-09-16
This post was last edited by linweihua6 on 2011-9-16 09:08. Why hasn’t the liquid level at the bottom of the tower risen since the slurry pump was stopped?
Reply #82011-09-16
Reply to 3# yiransunny: I’m sorry; I was reading quickly at that time and thought it was the preheating element of the backup pump that was leaking. Therefore, I suggest using crude oil for preheating, so that the preheating element won’t get worn out.
Reply #92011-09-16
Previously, when the solid content of our oil slurry was high, this kind of problem often occurred with the pre-heating line valves; there was no shutdown of the process, and the amount of reprocessed oil sent back to the tower was increased. It took 2 hours for the situation to be resolved after the liquid level reached its maximum level. The quality of the diesel remained normal, and in total, 3.5 hours were required to deal with the issue. Our maximum allowable time for dealing with such problems was originally 2 hours only
Reply #102011-09-17
Theoretically, it is feasible to stop the slurry pump for a short period of time; at a rate of 2 tons of slurry being discharged per hour, stopping it for 5 hours would result in only 10 tons of slurry, which should be sufficient to handle in the distillation tower. Even when the liquid level is full, oil and gas can still pass through, though with more resistance.

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