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How to detect the KCl content in acidic mother liquor water

2012-04-08View Original

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I have an acidic mother liquor that needs to be tested for its KCl content. Seek an analysis method.
Reply #22012-04-08
To determine the concentrations, chloride and potassium ions are measured separately; chloride can be determined by titration or ion chromatography, while potassium is determined by atomic absorption or flame photometry
Reply #32012-04-20
For high concentrations, chemical titration can be used: sodium tetraphenylborate is employed to determine potassium – \"Chemical World\", March 1955 issue
Reply #42012-04-20
In a solution, if potassium chloride is not the only dissolved salt, it is not appropriate to use terms related to the determination of potassium chloride; it is better to measure the concentrations of chloride ions and potassium ions separately. Method for detecting chloride ions: 1) Precipitation titration with standard silver solution; 2》Potentiometric titration of standard silver solution ; These two methods must eliminate interfering factors during chlorine determination ; 3》Ion chromatography ; 4》Chloride ion selective electrode method (low accuracy) ; Methods for detecting potassium ions: 1) Sodium tetraphenylborate titration method or gravimetric method ; 2》Ion chromatography ; 3》Potassium ion selective electrode method ; 4》Atomic absorption spectrometry ; 5》Atomic Emission Spectroscopy

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