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The outlet temperature of the distillation tower is negative

2017-10-22View Original

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I built a distillation column with ethylene flowing upward and propylene flowing downward; however, after it started operating, the temperature at the upper part became negative. I need help from experts
Reply #22017-10-22
If Aspen can run, there shouldn’t be any problems; it must be that you set the conditions incorrectly
Reply #32017-10-23
The pressure design is too low; it is recommended to increase the pressure so that, under conditions where the ethylene at the top of the tower reaches the specified purity, the dew point temperature is 40–50°C, thereby enabling condensation using condensate water. This system needs at least 10–15 bar.
Reply #42017-10-23
This post was last edited by zhxbkofkyo on 2017-10-23 at 15:58. It’s too difficult to try to use condensate water for condensation; it’s more reliable to use an ice machine for cooling. Also, there must be an issue with the pressure setting – it’s vacuum on the lower side. If the propylene temperature is over 100 degrees, the pressure is too low
Reply #52017-10-23
In Aspen simulations for distillation, it is assumed by default that the vapor at the top of the tower is condensed into a saturated liquid phase. At atmospheric pressure, ethylene has a very low boiling point; therefore, extremely low temperatures are required to cool it down, resulting in high costs in terms of cooling energy.
Reply #62017-10-23
Increasing pressure has little effect on temperature
Reply #72017-10-24
Are there any other low-boiling non-condensable gases in the system besides ethylene and propylene?
Reply #82017-11-01
Ethylene has a relatively low boiling point at atmospheric pressure; if there are other non-condensable gases in your system with even lower boiling points, then using a total condenser will result in a very low temperature at the top of the tower.

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