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I’m seeking help from experts: how can I reduce pressure fluctuations in the system when starting up hydrogen production for the first time and switching to cyclic feeding mode for gas generation?

2016-05-13View Original

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This post was last edited by tt12345ss on 2016-5-13 at 16:35.
Prerequisites:
1) Once vulcanization is complete, the hydrogenation reactor is removed and pressure is maintained; the desulfurization reactor then continues with the N2 circulation for temperature increase. The process flow is as follows: K3001A (compressor) —— F3001 (preheating furnace) —— R3001 (hydrogenation reactor) —— R3002 (desulfurization reactor) —— E3005 (start-up cooler) —— D3002 (for start-up purposes) —— K3001A.
2) Once conversion and medium-voltage reduction are complete, the process flow is as follows: K3001B (compressor) —— F3002 (conversion furnace) —— R3002 (medium-voltage reaction reactor) —— E3002 (cooling) —— D3004 (liquid separation); after that, three-stage cooling and liquid separation take place —— K3001B.
3) The overall cycle of the plant is as follows: K3001A (compressor) —— F3001 (preheating furnace) —— R3001 (hydrogenation reactor) —— R3002 (desulfurization reactor) —— F3002 (conversion furnace) —— R3002 (medium-voltage reaction reactor) —— E3002 (cooling) —— D3004 (liquid separation); after that, three-stage cooling and liquid separation take place —— K3001A (compressor).
Question A: When cycles 1) and 2) operate simultaneously, i.e., two separate cycles, how can this be changed to an overall cycle in order to minimize pressure fluctuations in the system? B: What impact will reducing the load on Unit B first and then changing the process cycle have on the system, and what effect will it have on the conversion catalyst? C: What impact will changing the process loop first and then reducing the load on Unit B have on the system, and what effect will it have on the conversion catalyst? D: Please ask an expert to provide a more specific plan for making the changes! !
Reply #22016-05-14
First, adjust the pressures of the two systems to be the same, and then changing the process will eliminate fluctuations.
Reply #32016-05-14
If the pressures of the two systems are adjusted to be the same, and if the load on unit B is reduced to change the process flow, will the fact that some of the gas does not flow pose any harm to the conversion catalyst?
Reply #42016-05-16
1. Balance the pressures of the two systems. 2. Change A to a large-loop process. 3. Reduce the load on machine B and shut it down.
Reply #52016-05-17
There is no need to rush to switch to a larger circulation cycle since no feed has been introduced yet. Wait until the desulfurization feed is available and its quality is verified, then connect it to the conversion system. After that, reduce the load on Unit B until it stops operating – this is the safest approach

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