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Incident of increased fine powder due to slurry pump switch-over. Recently, during the switch-over of the slurry pump in our facility, we observed a significant increase in the level of fine powder in the regenerator. The details are as follows: On 2024-06-11 at 9:30, the slurry circulation pump P2209A was switched to pump B; the switch-over was completed at 10:30; 2. At 9:55, it was observed that the particle size of the flue gas at the inlets and outlets of the three-spinner, as well as at the inlets and outlets of the desulfurization scrubber, increased simultaneously. Specifically, the particle size at the inlet of the three-spinner rose from 460 mg/m3 to 1066 mg/m3, while at its outlet it increased from 83 mg/m3 to 163 mg/m3. At the inlet of the desulfurization unit, the particle size increased from 74 mg/m3 to 142 mg/m3, and at its outlet it rose from 2 mg/m3 to 22 mg/m3. By 19:00, these values began to decrease gradually ; On June 12, 2024, the data at various points returned to normal levels. At 11:00, due to excessive gas-phase load on the backside, adjustments were made: the processing volume was reduced from 130 to 118 t/h, while the amount of slurry fed back for reprocessing increased from 14 to 22 t/h ; 4. The slurry taken from the desulfurization unit appeared quite turbid; there was a layer of catalyst at the bottom of the sediment, with a higher catalyst content than in normal slurry ; 5. Increase the amount of slurry discharged outside; at 16:00, a sample of the slurry was analyzed, showing a concentration of 4.4 mg/l, which is within the normal range ; During this period, no large-scale dosing or dosing removal operations were carried out, and the pressure drop in the regenerator and the pressure drop in the three spinners changed synchronously on multiple occasions ; The density at the regenerator cyclone inlet remains essentially unchanged ; It is certain that a large amount of fine powder was indeed carried to the three spinners ; Analysis: It is preliminarily inferred that due to the switching of the slurry pump, the catalyst deposited in the pipelines may have entered the two reactors along with the recycled oil slurry, resulting in a significant increase in fine powder; this was clearly evident at the inlets and outlets of the three spinners as well as in the desulfurization unit ; Question: My unit experienced a similar phenomenon in 2023 due to the switching of the slurry pump; the particle size of the flue gas increased significantly, but it returned to normal by the next day ; But this phenomenon does not occur every time the slurry pump is switched ; It has occurred occasionally in recent years; for example, it happened once in my device in 2023, and once on June 11, 2024. Under normal conditions, the warm-up line of the slurry pump is unobstructed, there is little catalyst accumulated in the pipelines, and any accumulated catalyst can only enter the regenerator through slurry reprocessing. The solid content in the slurry is not high, so it is impossible to generate large amounts of fine powder; this situation persists for a while, and normal operation is generally not restored until the second day ; What could be the reason for this?
Switching the slurry pump may cause the catalyst accumulated in the pipelines to be carried into the regenerator, thereby increasing the fine powder content. This phenomenon does not occur every time a switch is made; it appears occasionally and may be related to the specific way in which the pump is switched or to the accumulation of catalyst in the pipelines. .
This situation occurs occasionally; normally, the amount of catalyst accumulated in the pipelines is limited, and it can only enter the regenerator through the slurry, so it should not cause a significant increase in the amount of fine powder in the regenerator. However, the timing of such occurrences coincides, and there are no other major adjustments made, making it difficult to determine the cause.
Check it: first, there is leakage in the settler; second, the flow rate of the slurry is low and the circulation volume is small; third, the operation is unstable
Firstly, there is a problem of fine particles in your device – mainly fine dust. During prolonged operation, the preheating of the standby pump is relatively low and the flow rate is low, which leads to excessive accumulation of these fine particles. Fortunately, you can switch to another pump; but if this is done over an extended period of time, it might become impossible to start the pump again. In the future, regular switching should be carried out, and the maintenance room must thoroughly inspect the spin separation system inside the settler; resolving the issue completely is the key.
I think it might be the switching of the slurry pump that causes fluctuations in the liquid level at the bottom of the fractionation tower, which in turn affects the pressure in the reverse regeneration system and leads to changes in the operating conditions of the three spinners, resulting in a reduced separation efficiency.
There is no direct logical relationship; the fine powder is caused by catalyst wear and thermal decomposition.
I don’t agree with this claim. The amount of material reprocessed does affect the three spinners and the regenerator