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I often hear people talk about a “process package” – but what exactly does it include?

2021-07-01View Original

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Chemical process packages (complete technology packages) are the core of chemical production and play a crucial role in the chemical manufacturing process. So, what exactly does a chemical process package include? Which specialties are required to jointly complete the design of a process package? The development of a process package is a systematic project. It involves multiple specialties and disciplines, making it difficult to accomplish alone. Generally speaking, the development and design of process packages are carried out by various specialties such as research and development, chemical engineering processes, process systems, analysis and testing, automatic control, materials science, safety and health, and environmental protection, all working together to create the process package for that chemical product. What design documents should be included in the finished process package? The final deliverables of the package shall include an instruction manual, a process flow diagram (PFD), a preliminary piping and instrumentation diagram (P&ID), proposed equipment layout drawings, a list of process equipment, data sheets for process equipment (accompanied by simplified drawings of the equipment), a summary table of catalysts and chemicals, a summary table of sampling points, a materials manual (if required), a safety manual (covering occupational health, safety, and environmental protection), an operating manual (including an analytical manual), a physical properties data manual, and relevant calculation sheets. The quality control for the design of the process package is the same as the quality control requirements stipulated in the company’s design standards for all relevant disciplines at the basic design/preliminary design stage. Detailed specifications for the content and depth of the process package design 1 Instructions The process package design instructions constitute an important part of the process package design, and should include the following: a) Production methods, characteristics of the equipment ; It describes the advancement, reliability of the production methods employed in the process package design, as well as the characteristics of the equipment. b) Product name and scale, annual operating hours, and mode of operation of the equipment – operated in a three-shift-five-team or three-shift-four-team schedule, or other modes of operation. c) List the names of the various sections that make up the unit, in the order of the process sequence. d) List the names of the equipment and devices that generate the three types of waste, as well as the names, quantities, compositions, and emission forms of these wastes; include explanations regarding the comprehensive utilization and treatment of such wastes. (1) Design basis: List separately the names and specifications of the raw materials, catalysts, and chemicals. List the names and specifications of utility services such as water, electricity, gas, steam, etc., separately. (2) Process design: Describe the principles of the process, list the chemical reaction equations involved in the process (including primary and secondary reactions), and explain the catalysts used. In the order of the process sequence, the process flow is described in detail by sections and systems (tower system, reactor system, compressor system). For each section and system (tower system, reactor system, compressor system), the normal operating conditions at various key points are listed, such as temperature, pressure, flow rate, composition, and main control parameters. List the expected and guaranteed values for product specifications, production volume, and raw material consumption. List the main utility consumption indicators. For each section and system (tower system, reactor system, compressor system), the principles of process control are described in detail, and the process safety interlock system is also explained. The selection of key equipment such as reactors, main mass transfer devices, main heat exchange equipment, and pumps is explained in terms of structure, form, material selection, etc. 2 Drawings: Process Flow Diagram (PFD), along with a material balance sheet ; Piping and Instrumentation Diagram (P&ID) ; Proposed equipment layout diagram ; The recommended equipment layout plan should include the following: suggestions for the types of buildings and structures along with reference dimensions; the relative positions and elevations of the equipment (shown in proportion, without the need to indicate exact dimensions); the relative positions, elevations, or height differences of equipment with special requirements (exact dimensions must be specified); the names and tag numbers of all or the main equipment; and the relative locations of the control room and the main operation room. 3 Table: List of Process Equipment ; Process Equipment Data Sheet (with equipment diagram) ; Summary Table of Catalysts and Chemicals ; Summary table of sampling points (if required) 4 Safety manual (including occupational health, safety, and environmental protection) Provides a brief overview of the main contents of the safety manual, its purpose in being compiled, and its functions. Process description: Includes an explanation of the chemical principles and the process flow of the equipment. Detailed data on the basic physicochemical properties of raw materials, intermediate products, and final products, as well as information regarding fire, explosion, toxicity, etc., and the measures for controlling them. Measures and control methods taken to prevent accidents such as fires, explosions, and poisonings, based on the nature of the device. For example, regulations regarding ventilation, emergency exits, fire extinguishers, safety showers, eyewash stations, breathing equipment, and the provision of personal protective equipment. 5 Operation Manual (including the analysis manual, to be provided by the patent holder after all engineering designs are completed) Provides a brief overview of the main contents of the operation manual, its purpose in preparation, and its functions. Descriptions of chemical principles, plant process flows, and utility systems, along with reduced PFD and P&ID diagrams. List the recommended operating parameters for various units or systems (reactor systems, tower systems, compressor systems, etc.), as well as the effects of changing these parameters on the plant. It includes steps for conducting final inspections of equipment and piping mechanisms, procedures for lubricating valves and related mechanical components, steps for cleaning and purging equipment and piping, procedures for inspecting and calibrating instruments, and requirements for the commissioning and operation of pumps, compressors, and other equipment. Steps for driving, normal operation procedures, steps for normal and emergency shutdowns. Detailed normal and emergency shutdown procedures for process units and utility support systems. 6 Analysis Manual: Provides a brief overview of the main contents, purpose of compilation, and functions of the analysis manual, as well as the responsibilities, organization, and collaboration within the analysis department. A brief explanation of the basic requirements for sampling point design is provided, and the specific location, type of sampling point, analysis items, and analysis frequency for each sampling point in the entire system are listed in a sampling point summary table. The sampling procedures include the following aspects: safety measures for sampling operations, preparation of sampling containers, sampling steps as well as the preparation and processing of samples, and the techniques and methods for obtaining representative samples. List the analysis methods used for sampling and analysis of the entire plant, including those for raw materials and products, as well as the relevant analysis methods for various sections and systems of the plant. Development of process packages for chemical production processes. Chemical production processes mainly consist of two parts: reaction and separation. The reaction process is the core of chemical production, while the separation process is an important means to ensure product purity; both are essential. The task of the reaction process is to determine the reaction pathway and obtain the optimal reaction conditions through parameter optimization. When selecting the route and conditions, the following factors need to be considered comprehensively: yield, conversion rate, selectivity, energy consumption, safety, stability, medium corrosivity (which relates to material selection), the amount of waste generated, equipment investment, operating costs, etc. Common separations in chemical plants include gas-liquid separation, absorption, stripping, desorption, distillation, etc. Different separation methods are suitable for different operating conditions. A trade-off should be made based on the material composition and separation requirements.

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