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Azeotropic distillation dehydration with isopropanol

2018-05-08View Original

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Before the logistics B1-recyc connection to the mixer, it is shown that a certain amount of benzene flows out from the bottom of the azeotropic tower. But by integrating the mixer into the process, the benzene component in the entire tower disappears
Reply #22018-05-09
I haven’t encountered it yet; it seems too fantastical. If it is process development, why not use extractive distillation instead of heterogeneous azeotropic distillation? Extractive distillation is usually more promising.
Reply #32018-05-09
Well, I’ve learned something. It’s just that the graduation project requires the use of azeotropic distillation. When simulated with Aspen, the entire process can meet the requirements and converge without an azeotrope. I don’t know what the reason is.
Reply #42018-05-11
This system exhibits azeotropy; if the product meets the required standards without the use of a stripping agent, then there is a problem with the thermodynamic approach, as it is unable to predict the azeotrope temperature; Or there is a problem with the binary interaction parameter in the thermodynamic approach. Solution strategy: Use the selected thermodynamic method to predict the azeotrope point of IPA/W to see if it is possible to make an accurate prediction. If it cannot be predicted, use heat transfer mechanics methods, or re-estimate the binary interaction parameters using VLE experimental data.
Reply #52018-05-13
Thank you, the issue has been resolved. It was resolved by changing the calculation method for the shear flow

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