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Distillation reflux issue

2022-01-12View Original

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I have a question for everyone. When designing the system, I added a blind flange to the return pipe from the condenser to the reactor, as I thought that in the case of simple distillation, the condensed liquid wouldn’t flow back. However, my supervisor asked me to remove that blind flange. I would like to know when the condensed liquid will flow back into the reactor
Reply #22022-02-17
There’s no reason to install blind flanges at all. Generally, reflux takes place continuously; if blind flanges are used, how can reflux occur back into the reactor?
Reply #32022-03-22
This post was last edited by WuLìJù LǐLùn on 2022-3-22 at 15:53. Yours is a distillation kettle; as long as the non-condensable gases in the condenser need to return to the condenser for further cooling, they don’t flow back into the distillation kettle
Reply #42022-12-10
Under normal operating conditions, internal recirculation can be used to reduce solvent evaporation losses.
Reply #52022-12-12
For example, there is backflow dehydration (separation of oil and water, removal of water), with the solvent continuing to flow into the reactor, etc

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