Can a three-valve assembly be used for discharging material from a vacuum reactor?
Thread Content
As shown in the figure, this reactor is a vacuum reactor; it is necessary to take samples of the liquid inside the reactor at regular intervals for analysis. Using the traditional three-valve system, is it possible to take samples at the sampling port?
No, add an interface and connect it to the reactor; the gas phase needs to be connected as well
Check what your liquid level and vacuum degree are
Thank you all for your interest. I thought it couldn’t be released, but a professor from a university said it could be made available. Currently, while the equipment is being installed, I plan to modify its design by taking samples.
If the vacuum level isn’t high enough and the liquid level in your tank is sufficient, it can be taken out; if not, follow the suggestion from the second floor! The valve on the far right is connected to the top of the tank! But your approach requires releasing a lot of \"useless data\".
It can be retrieved now, but it’s not representative
It should be possible to remove it; it’s not representative. Also, if the pressure in the reactor is low, air will enter the reactor.
Adding a small sampling circulation pump is the most reasonable solution; it is a bit more expensive, but it resolves all the problems.