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The feed to the desolventizer tower increases, and the vacuum in the tower decreases

2022-08-18View Original

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The desolventizer tower is primarily used to remove most of the solvent from the material. Feed is introduced into the tower under flow control; the temperature at the bottom of the tower is 120°C. Butyl acetate, the solvent, is extracted from the top of the tower and recovered through cooling with circulating water and chilled water. The vacuum level is maintained at -0.093 to -0.095 MPa. During the first round of production, a feed rate of 5–6 m3/h had no effect on the vacuum level. Recently, a feed rate of 1–2 m3/h also does not affect the vacuum, but when the feed rate exceeds 4 m3/h, it affects the vacuum level, causing it to drop to around -0.089 MPa; however, the system’s pressure remains normal. Could you tell me what the reason is?
Reply #22022-08-18
Is it possible that the seasoning has caused a blockage?
Reply #32022-08-19
If the temperature at the bottom of the tower does not decrease, it is more likely that the two condensers at the top of the tower are not functioning properly – either there is not enough water for cooling, or the heat exchange efficiency of the heat exchangers is poor
Reply #42022-08-20
Check the condensation effect, examine changes in the temperature and flow rate of the cooling water in the circulation system, and verify whether the heat exchanger is clogged.
Reply #52022-08-28
Thank you. The pressure testing of the tower and the inspection of the pipeline for blockages showed no abnormalities; the cause is likely large fluctuations in feed volume and poor condensation efficiency
Reply #62022-08-28
Thank you. The pressure testing of the tower and the inspection of the pipeline for blockages showed no abnormalities; the cause is likely large fluctuations in feed volume and poor condensation efficiency

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