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Steps for commissioning a new diesel hydrofinishing unit – please help with the details

2015-10-12View Original

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Please help, write down the detailed steps for me. Skip pre-vulcanization; what should I do next? Please help!
Reply #22015-10-13
After pre-sulfidization is completed, passivation is required; at this point, water injection should begin. Once passivation is finished, the feed oil should be gradually adjusted, and the closed-loop circulation should be slowly shut down while feeding the material to the distillation unit, until the closed-loop circulation stops completely and all the material is fed to the distillation unit. Sample the product for analysis and adjust the parameters.
Reply #32015-10-14
After the high-temperature sulfidation of the catalyst was completed, the reaction system was cooled to 280 degrees, and straight-run diesel was used to replace the sulfided oil; the catalyst was passivated with straight-run diesel for 72 hours. During this period, cracking diesel was not allowed to be introduced, in order to prevent the reactor bed temperature from rising due to the high activity of the catalyst

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