Determination of the saturated solubility of silane in liquid ammonia
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I have a question for those who are experienced in this field: Has anyone ever measured the solubility of silane in liquid ammonia? Or experiments to determine the solubility of nitrogen or other gases in liquid ammonia are also possible. Whether it’s for enterprises or universities, I would appreciate your advice! Thank you! My contact information via WeChat or QQ: 9685238
I originally came here looking for answers, but found that almost no one offered any solutions. In light of this, as a tentative idea to stimulate further discussion, I have a rough proposal; I’m not sure if it can solve the problem, but I’d like everyone to consider it together. Solution: 1) Create a small pressure vessel with two openings, one for gas inlet and one for water inlet. 2) The pressure vessel is equipped with a sensor, a pressure gauge, and a temperature sensor (this can be omitted to save costs). 3) The vessel is filled with silane gas at a certain pressure, followed by the addition of a certain amount of liquid ammonia; after stabilization, it is measured how much the pressure inside the vessel has decreased. 4) Determine the dissolved amount of silane gas in liquid ammonia based on pressure changes.