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Problems with the methanol-water separation tower in low-temperature methanol washing

2021-02-17View Original

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Problems with the methanol-water separation tower in low-temperature methanol washing: Our methanol-water separation tower experiences significant fluctuations and cannot be controlled stably. I wonder how it is for others?
Reply #22021-02-17
The methanol-water separation tower mentioned by the poster is a common problem in the industry. In 2004, relevant personnel at Jiujiang Large Fertilizer raised the issue of the methanol-water separation tower. The tower suffers from issues such as corrosion, blockages, and overloading, which cause large fluctuations in its operation. As a result, the water content in the circulating methanol often exceeds the specified limits, which in turn exacerbates corrosion and blockages within the system, creating a vicious cycle. These tower trays generally use bubble-type trays (floating valves, guided floating valves, sieve trays, differential floating valves). . . ), it is not suitable for the operating conditions of the methanol-water separation tower.
Reply #32021-02-25
If it was normal before, analyze the changes in the composition of the shift gas entering the methanol wash
Reply #42021-02-26
It would be best to include a trend chart; there are large fluctuations, and it’s not possible to maintain stability – the scope for imagination is too wide
Reply #52021-03-04
Our operation is stable, without any fluctuations as mentioned above. It’s the tower wall that has been corroded and penetrated
Reply #62021-03-13
Stabilizing the tower temperature and pressure will make things much better
Reply #72021-04-06
First, set the temperature manually to a certain level, then identify the cause of the fluctuations. What should be done if no cause can be found?
Reply #82021-04-18
Generally, it’s the tray that’s blocked; start the tower once to check whether the tray is blocked or not. If there are still fluctuations, check whether your regeneration tower is clogged.

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