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How to deal with residual mud in the pot? It starts to clog the tower now; it flows in a liquid state when it’s hot, and turns solid when the temperature drops

2017-07-25View Original

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How to deal with residual mud in the pot? Now it’s starting to clog the tower; it flows in a liquid state when it’s hot, but turns solid when the temperature drops. Once it’s in a solid state, it won’t melt no matter how much heat is applied, and none of the solvents used can dissolve it.
Reply #22017-07-25
Let’s talk about what the main components are, and then have everyone help you find a solvent
Reply #32017-08-11
I don’t know what solvent to use; it doesn’t dissolve when heated in DMF, nor in THF. Propanone and acetonitrile have been tried as well

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