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Methanol water distillation tower

2018-10-17View Original

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The methanol content in the wastewater discharged from the methanol distillation tower of my company has suddenly increased. The temperature at the bottom of the tower is around 140°C, and the methanol concentration has risen to about 4%. What could be the reason for this, and how can it be adjusted?
Reply #22018-10-18
What is the pressure at the top of the tower? Is it too high?; Is there any abnormally high level of methanol in the feed?
Reply #32018-10-18
Check the tower pressure difference and temperature gradient to see if flooding has occurred
Reply #42018-10-29
Based on the phenomenon you described, the substandard quality of the residue at the bottom of the tower is likely due to an insufficient amount of steam rising inside the tower, which results in liquid leakage. The following measures can be taken to address this issue: 1. Reduce the feed rate; 2. Increase the heat load at the bottom of the tower ;
Reply #52018-11-07
What’s the tower pressure difference? Is there any drift phenomenon? Refeed the tower for operation; if the same issues occur, shut down the tower to check the overflow weir and other internal components of the tower.

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