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After flash evaporation of the feed to the distillation column, does the feed still enter the column for further flash evaporation?

2023-12-21View Original

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Hello, everyone: I encountered a problem during the ASPEN simulation. ① The reaction mixture (at 4.5 MPa) is either reduced in pressure to atmospheric pressure via a pressure relief valve before being fed into the tower as a gas-liquid mixture, or it is fed directly into the tower without going through a pressure relief valve; the feeding location remains the same. During hydraulic calculations, the diameter of the stripping section was found to be 2.7 m, while the diameter of the distillation section was 2.1 m; ② After being flashed in a flash tank at 4.5 MPa, the reaction mixture is fed as a gas phase and a liquid phase at atmospheric pressure; based on hydraulic calculations, the diameter of the stripping section is 2.1 m, and the diameter of the distillation section is also 2.1 m ; I would like to ask whether these two feeding methods are due to the fact that the reaction liquid in ① flashes inside the tower, resulting in an increase in the tower diameter. I don’t quite understand why it is the stripping section; could it be because flashing takes time, and as the feed liquid flows downward it keeps flashing, which causes the diameter of the stripping section of the tower to increase? ;
Reply #22023-12-21
In the design and operation of distillation columns, the conditions of the feed (such as temperature, pressure, and phase state) have a significant impact on the flow and mass transfer processes within the column. The two different feeding methods you mentioned – feeding directly into the tower by reducing the pressure to atmospheric levels using a pressure relief valve, and feeding after flash separation in a flash tank followed by phase separation – result in differences in flow patterns and separation efficiency within the tower. The reasons are as follows: 1. Direct pressure reduction before entering the tower: In your first scenario, when the high-pressure reaction mixture is reduced to atmospheric pressure via a pressure regulator, some of the liquid will flash immediately due to the drop in pressure. This process generates a large amount of steam inside the tower, thereby increasing the gas flow rate in the stripping section. If the feed location is near the stripping section, a large amount of steam requires that the stripping section have a larger diameter in order to handle higher gas velocities and prevent flooding or other flow problems within the tower. 2. Feed after separation in the flash tank: In the second case, the flashing process is carried out outside the tower. In this way, most of the vaporization occurs outside the tower, entering the tower in gas and liquid forms respectively. Therefore, the gas-liquid flow conditions inside the tower are more stable, and the gas flow rate is likely to be lower than when the gas enters the tower directly after pressure reduction, as part of the gas has already been separated. This may explain why, in this case, the calculation results show that the diameter of the stripping section can be kept the same as that of the distillation section. Indeed, as you guessed, in the first case, liquid is continuously flashing during the flow process; this occurs inside the tower, especially in the stripping section, and therefore a larger tower diameter is required to handle the increased two-phase flow rate. In the second case, since flashing has already taken place outside the tower, the gas-liquid flow load inside the tower is relatively low; therefore, a tower of the same diameter can be used for treatment. In summary, the variation in tower diameter indicates the effect of the two different feeding methods on the hydraulic performance of the distillation column. Choosing the correct feeding method and designing the tower diameter are key to ensuring the smooth progress of the distillation process. In practice, it is usually necessary to consider various factors such as energy consumption, operational flexibility, equipment costs, and process stability in order to select the most suitable feed method and design parameters for the column. .

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