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How to determine the esterification rate?

2016-11-03View Original

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We have worked with many fiber manufacturing companies, and the esterification rate is a parameter that receives significant attention in production. Moreover, almost all of these companies use continuous reaction processes, so it is extremely valuable to be able to monitor the esterification rate in real time. Two methods for detecting the esterification rate: The first method involves making no modifications to the reaction vessel (since polymerization vessels usually have jackets and are not suitable for having openings); as long as there is a gas outlet for the gas-phase reflux process on the vessel, it is sufficient to measure the change in gas-phase temperature, along with the change in the temperature of the material ; The second method involves creating a bypass in the pipeline connecting the reactors, installing a differential pressure transmitter, and then taking into account changes in the material temperature to carry out modeling. Of course, comparatively speaking, the second method is a bit more accurate than the first. Since it is a non-standard product, the specific procedures need to be determined based on the operating conditions. What methods do people use to determine the esterification rate? Welcome everyone to discuss and exchange ideas; thank you! !
Reply #22016-11-03
I wonder what your name is? I can send you the technical specifications, which will provide more details
Reply #32016-11-04
An esterification rate calculation model was developed by East China University of Science and Technology before, but it is not universal. At the current stage, it is not possible to obtain accurate values by calculating using parameters such as temperature, liquid level, and reflux
Reply #42016-11-04
Here, we collect signals from the field such as temperature, pressure, flow rate, and density; then we perform model calculations to determine the esterification rate using methods based on boiling point elevation or heat balance
Reply #52016-11-05
Has it been actually used in plants with different polyester production processes? Send some materials for me to learn from, zjnfxxh@126.com
Reply #62016-11-07
Okay, it has been sent. Please make sure to check it.
Reply #72017-02-27
I wonder what the actual measurement is? Could you send some materials? Thank you! luliw@163.com

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