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Discussion on some questions regarding the operation process of the roughing tower

2020-08-02View Original

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Our unit has a roughing tower primarily used for separating trichlorosilane and silicon tetrachloride. Operating pressure: 0.2 MPa. The temperature of the reflux tank is controlled at around 40 degrees. However, the vent at the top of the tower remains open at about 20% at all times. How to operate or adjust in order to maintain stable tower pressure while closing or reducing the anti-backflow valve. Reduce the waste from venting trichlorosilane.
Reply #22020-08-02
The most economical approach is to gradually reduce the heat source at the bottom of the tower, until the pressure relief valve at the top is closed to about 5% of its opening; maintaining an appropriate degree of opening is necessary to ensure unobstructed flow in the pipelines
Reply #32020-08-03
After reducing the steam volume, the feed rate fails to meet the requirements. It increases after extraction from the tower bottom. The tower top output is affected.
Reply #42020-10-20
OP, can we add each other on QQ? Let’s discuss the production process of trichlorosilane together. Thank you. QQ 455732743

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