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In the low-pressure urea production system using the carbon dioxide stripping method, the pressure is high, but the concentration of ammonium methylate solution is not high – could it be that the packing in the distillation tower is damaged?

2015-07-18View Original

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In the low-pressure urea production system using the carbon dioxide stripping method, the pressure is high, but the concentration of ammonium methylate solution is not high – could it be that the packing in the distillation tower is damaged? Was partially damaged packing blown into the condensation system, causing the tubes to get clogged?
Reply #22015-07-18
Is it caused by partial crystallization in the low-pressure condensation system?
Reply #32015-07-19
There is no crystallization; the temperature difference remains above 11°C, with no significant changes. Keeping the inlet water temperature at 60°C prevents crystallization. Currently, the concentration of ammonium hydroxide solution does not exceed 60
Reply #42015-07-20
It’s necessary to check the distillation tower feed distributor; photos would be helpful, and fellow sailors can assist with the analysis.
Reply #52015-07-29
This post was last edited by WJHSWSW on 2015-7-29 at 13:49. Check whether there is cross-feeding in the stripper Is the liquid level in the low-temperature coolant sump too high? To be more specific, is it the pressure in the distillation tower that is high, or is it the gas phase pressure in the low-pressure liquid level tank that is high? Easy to analyze.
Reply #62015-08-06
When the operating conditions are stable and the indicators are normal. Heat exchange of circulating water can be considered; high temperatures result in a reduced flow rate of the circulating water, which leads to insufficient condensation and an increase in pressure in the low-pressure system.
Reply #72015-08-19
The temperature difference in the low-pressure water is 11°C, which seems high; ours is 3.5°C. Is the flow rate of the low-pressure water too low? Check the low-flow rate and the operation of the pump?

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