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What are the precautions for catalyst heating reduction?

2015-11-03View Original

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What are the precautions for catalyst heating reduction?
Reply #22015-11-03
The most common ones are the three principles. That is, the three lows: low-temperature water discharge, low-hydrogen reduction, and low-load operation after reduction ; Three prohibitions: It is not allowed to increase hydrogen pressure and temperature simultaneously, water must not be introduced into the synthesis tower, and water discharged at high temperature for extended periods is prohibited ; Three controls: control the water output per hour, the hydrogen addition per hour, and the heating rate per hour ; Three stabilities: hydrogen supplementation stability, effluent stability, and temperature elevation stability. Next, when taking water on-site, one should stand in a safe location with a favorable wind direction; the water should be weighed accurately and promptly, and the drained water should be poured in a safe place. The control system is used to strictly regulate the temperature of the bed layer – if an increase in temperature is detected, the steam supply should be reduced, and if necessary, emergency nitrogen flushing should be carried out for displacement. There are two types of temperature-raised reduction: one is high-hydrogen reduction, which results in good catalyst activity after the reduction process, but it is difficult to carry out; the other is low-hydrogen reduction, which is simple to operate but takes longer time.

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