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What are the testing methods for vanadium content?

2015-11-10View Original

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I have been working on the measurement of vanadium recently, and I’m interested in knowing what are the current mainstream methods for analysis. Apart from graphite furnace atomic absorption spectrophotometry and tantalum reagent extraction spectrophotometry, are there any other analysis methods that can be used in laboratories without the need for highly advanced equipment? Thank you, experts; please help
Reply #22015-11-10
Redox titration and complexometric titration are suitable for determining percentage content
Reply #32015-11-10
Taking advantage of the oxidizing property of pentavalent vanadium, redox titration can be used for detection; the author can look it up in the volumetric analysis section of the \"Manual of Analytical Chemistry\". For the colorimetric detection of vanadium, there are quite a number of references available; its sensitivity is not lower than that of atomic absorption, and its accuracy is certainly better than that of atomic absorption. In complexometric titration, vanadium is a high-valent ion with multiple valence states, so the conditions for such titration require consideration of the appropriate acidity level as well as the masking of interfering ions. Ion chromatography can also detect vanadium compounds.

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