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Seek purification processes for industrial sodium carbonate and ammonium chloride to produce refined reagent-grade products. Those who know the way, please send it over

2018-05-18View Original

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Seek purification processes for industrial sodium carbonate and ammonium chloride to produce refined reagent-grade products. Those who are knowledgeable please contact and leave a message
Reply #22018-05-18
This post was last edited by mkp369 on 2018-5-21 09:33. Both of the products mentioned above are produced using the ammonia-alkali process; the main impurity in sodium carbonate is chloride ions, while the main impurities in ammonium chloride are sodium ions and sulfate ions. How can these impurities be removed?
Reply #32018-05-18
Refining these two products is not that difficult.
Reply #42018-05-18
The key is cost-effectiveness, and multiple crystallizations can solve this problem.
Reply #52018-05-18
Multiple crystallizations result in low yields, poor economic efficiency, and are also harmful to the environment
Reply #62018-05-18
This post was last edited by mkp369 on 2018-5-21 09:36. The chlorine content in industrial-grade sodium carbonate ranges from 0.3% to 0.7%; only about one-tenth purification can be achieved through a single recrystallization process. The required level for reagents is 0.002%, and at least three recrystallizations are necessary.
Reply #72018-05-18
Why was only the crystallization method considered?
Reply #82018-05-19
What other options are there besides crystallization?
Reply #92018-05-21
Ammonium chloride is a double-alkali product, not an ammonia-alkali product.
Reply #102018-05-21
The chlorine content in industrial-grade sodium carbonate can be controlled to well below 0.3%.

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