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Latest synthesis techniques for benzoyl chloride

2019-04-15View Original

Thread Content

At present in China, benzoyl chloride is produced through batch reactions in reactors, using trichlorobenzene and benzoic acid as raw materials under the catalysis of ferric chloride or zinc chloride; the amount of residue resulting from these reactions is about 2–3%, and this residue consists of high-chlorine tar. Due to the high chlorine content, the cost of treating such hazardous waste is very high, which is why no one is willing to take it on; A new synthesis technique has now been successfully tested: trichlorobenzene and benzoic acid are mixed in the theoretical ratio, heated to a liquid state, and then continuously fed into a specially designed reactor. The use of a solid composite catalyst ensures efficient and stable reactions, resulting in improved product quality. The key advantage is that this method enables continuous production with almost no residual waste; the reaction mixture only needs to be decolorized after processing. After several batches of testing, the catalyst lost almost no weight, allowing it to be used repeatedly over a long period of time.
Reply #22019-05-30
Is there a more detailed introduction? Additionally, what is the amount of 31% hydrochloric acid produced as a by-product in both methods?
Reply #32019-05-30
The amount of hydrochloric acid produced as a by-product remains essentially unchanged; everything proceeds in accordance with the reaction equations. The main advantage is the achievement of continuous processing, which improves yield and quality while reducing hazardous waste by 80%.
Reply #42019-05-31
How much 31% hydrochloric acid is produced as a byproduct per ton of benzoyl chloride?
Reply #52019-07-25
Does anyone know where I can find the technical process packages for trichlorobenzene or benzoyl chloride?
Reply #62019-07-25
It’s better to create a topic yourself, so that not many people will be able to see the replies
Reply #72019-07-26
Thank you! It has been posted separately! But still, no one replied! :'(
Reply #82019-07-26
Where is your friend from? Please contact me.
Reply #92020-06-03
Hello, I am interested in collaborating with you. My contact number: 15996454916
Reply #102020-06-03
Hello, I am interested in collaborating with you. Contact number: 15996454916, Pan
Reply #112021-09-27
Hello, I have experience in the process of producing chloromethane using hydrochloric acid. We could get to know each other and work together; my WeChat ID is 77968361. Thank you

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