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Seeking help with the separation issue in a distillation column using a chloroform-ethyl acetate system

2020-06-06View Original

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I would like to ask how to separate a chloroform-ethyl acetate mixture by distillation. Chloroform has a boiling point of 61°C, while ethyl acetate has a boiling point of 77°C; the two form an azeotrope with a boiling point of around 78°C℃; Based on the literature, operations such as extractive distillation and azeotropic distillation have been tried, but the results were not satisfactory; only one relevant paper was found ; I would be extremely grateful if anyone has conducted relevant research.

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