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Briefly describe the role of the reflux liquid in the distillation separation process?

2015-10-09View Original

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Briefly describe the role of the reflux liquid in the distillation separation process?
Reply #22015-10-10
As the reflux liquid descends, it mixes with the rising gas phase and absorbs heat. Some of the volatile components in the reflux liquid absorb this heat and rise along with the gas phase, while the less volatile components remain in the reflux liquid as it continues to descend. As a result, the concentration of volatile components in the gas phase inside the tower increases, and the concentration of heavier components in the reflux liquid also increases. In one sentence: Increasing the return flow can effectively improve product purity! But in actual production, the reflux liquid is mainly controlled comprehensively based on specific process requirements and energy consumption! Manager Ge from Yantai Zhi Chutian Da Precision Distillation Equipment Engineering Technology Co., Ltd.; Phone: 15753506807; Email: geyeflyh@163.com
Reply #32015-10-10
During the distillation process, the vapor generated by heating the mixture is drawn out from the top of the tower and enters the top condenser. Here, the vapor condenses (or partially condenses) into a liquid; part of this condensed liquid is returned to the top of the tower and flows downward along the tray surfaces, and this liquid is known as reflux ; Another portion of the condensate (or uncondensed vapor) is taken from the top of the tower as a product. As the reflux liquid flows downward along the tray, it undergoes multiple instances of partial vaporization and partial condensation in contact with the steam that is continuously vaporizing and rising inside the tower; this is a process of mass exchange, which increases the concentration of high-boiling-point components in the liquid returning back. Recirculation is a necessary condition for mass transfer through gas-liquid phase contact; without such phase contact, mass exchange cannot take place. Of course, the difference in the volatility of the components remains the basis of the distillation process.

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