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Factors affecting melting point

2015-11-12View Original

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We currently produce a product that appears in the form of crystalline particles. One of the key specifications for this product is its melting point, and strict requirements are imposed on this value. When analysts use melting point detectors to measure it, several problems arise: 1. For products from the same batch, the results obtained by different analysts differ by around 1 degree; 2. After drying, the test comes back positive; yet when it is processed together, another test is conducted and it turns out to be negative again. What are the specific operating procedures for Haiyou melting point, and what is the allowable error range? Which is more accurate, the automatic reading or the manual reading of a melting point apparatus?
Reply #22015-11-13
Melting point determination requires precise temperature control, and there are strict regulations regarding the rate of temperature increase. For both automatic and manual melting points, as long as the procedures are followed properly and the operator is skilled enough, there will be no significant discrepancies in the measurement results. But the main factor affecting the melting point of a pure substance is purity. When impurities are present, the melting point generally decreases.

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