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Problems with distillation towers

2022-02-20View Original

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Dear experts, what is the difference between drawing the liquid phase from the bottom of the distillation column reboiler and drawing it at a certain distance above the bottom of the column? Does this make any difference in terms of separation efficiency? And why is the internal structure of the tower bottom different?
Reply #22022-02-20
1. “What is the difference between drawing the liquid phase from the bottom of the distillation column reboiler and drawing it at a certain distance above the bottom of the column? Does this difference have an effect on separation?” ”. A reboiler is a device that converts the liquid at the bottom of the column into steam, which is then used as rising vapor for distillation together with the liquid flowing downward. 2. “And why is the internal structure of the tower bottom different?” ” Due to process requirements, the internal structure of the tower designed is different. There are various types of tray plates, such as floating valve trays, bubble cap trays, sieve trays, and structured packing. When learning such processes, it’s necessary to make distinctions; there’s no one-size-fits-all approach. To understand such a process, relevant explanations are also needed as a reference. For reference.
Reply #32022-02-20
The materials I’ve seen do not provide any explanations on this aspect; they all refer to plate towers. Since it is an ethane removal tower as well, the location where the liquid is drawn from the reboiler at the bottom of the tower varies – in most cases it is at the bottom of the tower, while in some special cases it is slightly above that point
Reply #42022-02-20
And I want to ask, what are the advantages of this liquid introduction method?
Reply #52022-02-22
At the very bottom is the drain port, which is also considered likely to get clogged if there are solids present. By shifting this area, the liquid phase that enters the reboiler is a cleaner process fluid; of course, the level gauge outlet must be above this point, as otherwise dry burning may occur and no vapor can be generated
Reply #62022-02-22
Generally, it is rare to use liquid drawn directly from the lowest part of the bottom of the boiler as a reboiling medium, as considerations regarding the purity of the medium and the efficiency of reboiling lead to liquid being drawn from above the bottom of the boiler instead. The method of drawing liquid from a higher position that you suggested is also feasible, but in order to prevent the liquid level in the tower from dropping too low and resulting in insufficient liquid being drawn, collectors and overflow plates are used to ensure that liquid overflows to the bottom of the tower only when enough liquid is available in the reboiler to allow for proper liquid withdrawal
Reply #72022-02-23
The bottom is for extraction, while the sides are mainly used for reboiler siphoning.

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