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Antimony pentachloride reactor type?

2017-10-23View Original

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Help: Does anyone know the method for preparing antimony pentachloride (SbCl5)? Currently, antimony blocks are placed in a reactor and chlorine gas is passed through them; an external circulating water pipeline is used to obtain antimony pentachloride. But in this case, it’s very difficult to control the reactor temperature; the introduction of chlorine is controlled by a needle valve, which results in a long catalyst preparation time and makes control difficult. I’m hoping someone can provide information on this topic
Reply #22017-10-24
In intermittent reactions, the needle valve can be used so that it stops operating when the temperature becomes high, and resumes operation once the temperature drops
Reply #32017-11-07
I hope there will be good reactor designs that can operate in a continuous manner
Reply #42018-01-27
This post was last edited by hywtg on 2018-2-2 19:47. Do you work with F11? I can handle the entire production line, including the antimony pentachloride reactor; please contact me via private message on phone.
Reply #52018-01-27
This post was last edited by hywtg on 2018-3-11 20:19. You can contact me at: 151846017**

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