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The micro-oxygen meter has a too large error compared to the manual value

2019-09-29View Original

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Process: Pressure swing adsorption; Equipment manufacturer: Shanghai Ruiqi. Problem description: In August 2019, the nitrogen production system was shut down due to a reduction in the amount of nitrogen used by the upstream units. Before shutdown, the production rate was 800–900 standard cubic meters per hour, with a purity level of 99.98%. After it was restarted a month later, the purity level fluctuated between 91% and 96%, and these fluctuations became more pronounced as the flow rate increased; the lowest purity level reached 99.89%. The sealings of the exhaust valves in both towers were damaged, and they were replaced today. The purity sensor as well as the micro-oxygen detector were also replaced. After these replacements, when the system was started up, the purity level was 99.98% at a production rate of 400 standard cubic meters per hour, with a micro-oxygen level of 400 ppm. However, manual analysis indicated a level of 800 ppm. What could be the reason for this, experts?
Reply #22019-09-30
Manual sampling may result in higher values in trace analysis, while online instruments can use standard gases to check for any deviations.
Reply #32019-09-30
There is a significant difference between manual analysis and instrument-based testing; it is recommended to send the micro-oxygen meter for calibration, so that the oxygen content can be measured accurately thereafter.
Reply #42019-09-30
Okay, thank you. I’ll prepare a standard sample this afternoon
Reply #52019-09-30
Okay, thank you. I’ll prepare a standard sample this afternoon

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